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SPHERICAL INDENTATION OF SiC...

by Andrew A Wereszczak, Kurt E Johanns
Publication Type
Conference Paper
Book Title
Ceramic Engineering and Science Proceedings
Publication Date
Page Numbers
43 to 57
Volume
27
Issue
7
Conference Name
30th International Conference and Exposition on Advanced Ceramics and Components
Conference Location
Cocoa Beach, Florida, United States of America
Conference Sponsor
American Ceramic Society
Conference Date
-

Instrumented Hertzian indentation testing was performed on several grades of SiCs and the results and preliminary interpretations are presented. The grades included hot-pressed and sintered compositions. One of the hot-pressed grades was additionally subjected to high temperature heat treatment to produce a coarsened grain microstructure to enable the examination of exaggerated grain size on indentation response. Diamond spherical indenters were used in the testing. Indentation load, indentation depth of penetration, and acoustic activity were continually measured during each indentation test. Indentation response and postmortem analysis of induced damage (e.g., ring/cone, radial and median cracking, quasi-plasticity) are compared and qualitatively as a function of grain size. For the case of SiC-N, the instrumented spherical indentation showed that yielding initiated at an average contact stress 12-13 GPa and
that there was another event (i.e., a noticeable rate increase in compliance probably associated with extensive ring and radial crack formations) occurring around an estimated average contact stress of 19 GPa.