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Probing orientation information using 3-dimensional reciprocal space volume analysis...

by Christopher M Fancher, Christina M Hoffmann, Matthias D Frontzek, Jeffrey R Bunn, Edward A Payzant
Publication Type
Journal
Journal Name
Review of Scientific Instruments
Publication Date
Page Number
013902
Volume
90
Issue
1

The crystallographic texture of polycrystalline materials is the result of how these materials are processed and what external forces materials have experienced. Neutron and X-ray diffraction are standard methods to characterize global crystallographic textures. However, conventional neutron and X-ray texture analyses rely on pole figure inversion routines derived from intensity analysis of individual reflections or powder Rietveld analysis to reconstruct and model the orientation distribution from slices through reciprocal space. In this work, we describe an original approach to directly probe the crystallographic texture information of rolled aluminum from the intensity distribution in 3-dimensional reciprocal space volumes measured simultaneously. Using the TOPAZ time-of-flight Laue neutron diffractometer, reciprocal space analysis allowed determination of “pole spheres” with <1° angular resolution. These pole spheres are compared with reconstructed pole figures from classic texture analysis.