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Fracture Toughness and Slow Crack Growth Behavior of Ni-YSZ and YSZ as a Function of Porosity and Temperature....

by Miladin Radovic, Edgar Lara-curzio, George Nelson
Publication Type
Conference Paper
Journal Name
Ceramic Engineering and Science Proceedings
Publication Date
Page Numbers
373 to 381
Volume
27
Issue
4
Conference Name
the 30th International Conference & Exposition on Advanced Ceramics & Composites
Conference Location
Cocoa Beach, Florida, United States of America
Conference Sponsor
The American Ceramic Society
Conference Date
-

In this paper we report on the fracture toughness of YSZ and Ni-YSZ and slow-crack growth behavior of Ni-YSZ at 20C and 800C. Results are presented for tests carried out in air for YSZ and in a gas mixture of 4%H2 and 96%Ar for Ni-YSZ containing various levels of porosity. The double-torsion test method was utilized to determine the fracture toughness from the peak load obtained during fast loading test specimens that had been precracked, while crack velocity versus stress intensity curves were obtained in the double torsion using hte load relaxation method. It was found that fracture toughness of these materials decreases with temperature and int he case of Ni-YSZ it also decreases with increasing porosity. The effect of temperature and microstructure, which was characterized by Scanning Electron Microscopy, on the fracture behavior of these materials, is discussed.