July 2016

ORNL Report

Manufacturing Demonstration Facility: Low Temperature Materials Synthesis

By:
Graham, David E; Moon, Ji Won ; Armstrong, Beth L; Datskos, Panagiotis G; Duty, Chad E; Gresback, Ryan G; Ivanov, Ilia N; Jacobs, Christopher B; Jang, Gyoung Gug ; Jellison Jr, Gerald E; Joshi, Pooran C; Jung, Hyunsung ; Meyer III, Harry M; Phelps, Tommy J
Publication Date:
July 2016

Abstract

The Manufacturing Demonstration Facility (MDF) low temperature materials synthesis project was established to demonstrate a scalable and sustainable process to produce nanoparticles (NPs) for advanced manufacturing. Previous methods to chemically synthesize NPs typically required expensive, high-purity inorganic chemical reagents, organic solvents and high temperatures. These processes were typically applied at small laboratory scales at yields sufficient for NP characterization, but insufficient to support roll-to-roll processing efforts or device fabrication. The new NanoFermentation processes described here operated at a low temperature (~60 °C) in low-cost, aqueous media using bacteria that produce extracellular NPs with controlled size and elemental stoichiometry. Up-scaling activities successfully demonstrated high NP yields and quality in a 900-L pilot-scale reactor, establishing this NanoFermentation process as a competitive biomanufacturing strategy to produce NPs for advanced manufacturing of power electronics, solid-state lighting and sensors.