Beam current effect as a potential challenge in SEM-EBSD in situ tensile testing

Abstract

In situ mechanical tensile tests coupled with electron backscatter diffraction (EBSD) analysis were conducted using specimens of two 304L steels with ~8 and 10.4% Ni content, respectively. Twinning was observed in steel with 10.4% Ni content, whereas steel with 8% Ni content demonstrated martensitic transformation. Testing showed that the kinetics of martensitic transformation in steel with 8% Ni content was influenced by the electron beam current used during EBSD scans. Continuous scanning using 32 nA nominal beam current led to suppression of the phase instability in the near-surface layer, but acceptable comparable-to-the-bulk results were obtained using 8 nA beam current. The exact mechanism of the beam current role is unclear, but it appears to be neutral regarding Kernel Average Misorientation behavior and deformation-induced twinning.