Spatially resolved strain measurements in Mo-alloy micropillars by differential aperture x-ray microscopy...

Spatially resolved strain distributions in the NiAl matrix and the ~550-nm Mo fibers of a NiAl-Mo eutectic were investigated by micro-beam X-ray diffraction. Position sensitive d-spacings for the individual phases were obtained from Laue patterns. For embedded Mo fibers, the measured elastic strain is consistent with the predicted thermal mismatch strain between the NiAl and Mo phases. However, when the NiAl matrix is etched back to expose Mo micro-pillars, the d-spacing increases to that of unconstrained Mo, indicating release of the compressive residual strain in the Mo fibers.