Oral Presentation 1-07

 

A Depolymerization Kinetics Model

For the Degradation of Hemicellulose

 

Todd Lloyd, Charles E. Wyman

 

Thayer School of Engineering

Dartmouth College

8000 Cummings Hall

Hanover, New Hampshire 03755

 

Telephone:  (603) 646-3193; Fax:  (603) 646-2277; E-mail:  Todd.Lloyd@Dartmouth.edu

 

Pretreatment has been shown to be the single most expensive processing step in the conversion of lignocellulosic biomass to fuels and chemicals.  Although the importance of pretreatment processing is universally acknowledged, a fundamental understanding of pretreatment mechanisms has been elusive.  For over 50 years the most commonly used models have been based on first order homogenous kinetics, or some variation.  In the case of hemicellulose degradation and solubilization during pretreatment, these models provide a useful fit of experimental data but suffer from some inconsistencies.  This paper describes an alternative kinetic model based on a depolymerization mechanism that assumes hemicellulose linkages are broken (and subsequently hydrolyzed) at random.  This creates oligomers with a distribution of chain lengths, with their concentrations at any time determined in a statistical manner.  The model is compared to pretreatment data from various researchers and other models.  The prediction of oligomers that may be solubilized during hydrolysis is emphasized.

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