WASTE R&D AT ORNL
   
   This article also appears in the Oak Ridge National Laboratory
   Review (Vol. 25, No. 2), a quarterly research and development
   magazine. If you'd like more information about the research
   discussed in the article or about the Review, or if you have any
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   In the past few years efforts to clean up hazardous waste at sites
   across the country, including Department of Energy facilities, have
   increased dramatically. Vast economic and personnel resources are
   being devoted to environmental restoration. Sometimes problems can
   be solved quickly using available techniques; however, solving many
   old environmental problems requires new methods and technologies.
   Creating these new approaches is the task of the Office of
   Technology Development (OTD) within DOE's Office of Environmental
   Restoration and Waste Management.    
   
   The success of this task depends to a considerable degree on
   maintaining open lines of communication between OTD and its
   counterparts, the Office of Environmental Restoration and the
   Office of Waste Operations. These organizations are involved in the
   nuts and bolts work of restoration, remediation, and waste
   management, often responding to crisis situations. During the
   course of this work, some areas are found to have cleanup and waste
   management needs that cannot be met with existing technologies.
   OTD's mission is to be attentive to these areas, seek out possible
   solutions, and nurture their development so they can be implemented
   in the field.    
   
   At ORNL, innovative environmental restoration and waste management
   techniques for OTD are being developed in the following areas:
   
        - Characterization--developing advanced models, field
          measurement and sensing methods, and data acquisition and
          analysis systems for mapping and determining the contents of
          a waste site;
   
        - Bioremediation--developing microorganisms to "eat" or
          otherwise stabilize selected organic contaminants, such as
          trichloroethylene (TCE) and polychlorinated biphenyls (PCB),
          and inorganic species, such as uranium and lead, in situ (in
          place) or in process;
   
        - Treatability--developing methods for treating soils
          contaminated with volatile organic compounds and low levels
          of radioactive substances; 
   
        - Robotics--developing robotic systems and remote technology
          to characterize and clean up waste without exposing workers
          to a hazardous environment;
   
        - D&D--decontamination and decommissioning of metals and
          concrete to assist in disassembling old facilities and in
          replacing several major facilities in the Defense Programs
          Reconfiguration;
   
        - Transportation--performing evaluations of transportation
          needs for on-site and off-site transfer of hazardous and
          mixed waste (hazardous and radioactive waste combined); and
   
        - Technology transfer--promoting the transfer of technologies
          developed at ORNL that potentially could improve program
          effectiveness, reduce costs, and save time for federal
          agencies, industry, academia, and the international
          community.
   
   All these activities involve developing new remediation and waste
   management methods or modifying existing techniques to create
   cost-effective, energy-efficient waste-minimization technologies. 
   
   
   CHARACTERIZATION    
   
   Finding more economical ways to clean up soil and groundwater
   contaminated by radioactive and hazardous chemicals is a priority
   in environmental restoration and waste management. The first step
   toward reducing the cost of cleaning up sites is reducing the cost
   of collecting and analyzing soil and groundwater samples. The
   process of collecting and analyzing samples is not only costly, but
   it also delays cleanup efforts because of the time required to
   obtain results. The Office of Technology Development is currently
   supporting a number of projects at ORNL addressing these problems. 
      
   
   For example, ORNL researchers Marcus Wise, Cyril Thompson, and Mike
   Guerin, all of the Analytical Chemistry Division, have developed a
   portable, real-time, direct-sampling ion-trap mass spectrometer
   that can detect hazardous organic compounds at extremely low
   concentrations. This device reduces sample processing time to less
   than half that required using conventional analytical methods (see
   the article on "New Waste Technologies" in this issue).      
   
   The improved Derivative Ultraviolet Absorption Spectrometer (DUVAS)
   system developed by John Haas of the Health and Safety Research
   Division measures groundwater contamination directly and, as a
   result, is able to more accurately characterize any such
   contamination. The system may have additional applications in the
   monitoring of manufacturing discharges and chemical process streams
   (see the article on "New Waste Technologies" in this issue).     
   
   The colloidal borescope previously developed by Tom Cronk and Pete
   Kearl, both of ORNL's Grand Junction, Colorado, office, is being
   adapted to measuring the velocity of groundwater flow. This
   instrument offers the potential for improved site characterization,
   design of faster and more cost-effective remediation strategies,
   and improved monitoring of the remediation process. Meanwhile,
   nondestructive assay and nondestructive examination methods using
   a linear accelerator have been developed for characterizing
   remote-handled transuranic (RH-TRU) waste by Fred Schultz of the
   Office of Environmental and Health Protection Compliance.     
   
   Tuan Vo-Dinh of the Health and Safety Research Division is
   developing a luminescence spot test for rapid screening of soils to
   find out if they contain PCBs. In this technique, the presence and
   concentration of PCBs adsorbed on chemically treated filter paper
   and exposed to light are determined by detecting and measuring
   their resultant luminescence. Advantages of the technique are that
   the simple instrumentation can be easily set up and used in the
   field and that it can analyze samples more rapidly and at a lower
   cost than conventional methods.    
   
   Some effort at ORNL has been devoted to developing technologies for
   analyzing air, water, and soil in place, thus reducing considerably
   the cost, time, and hazards associated with extracting,
   transferring, and analyzing contaminated samples.  
   
   Haas has been building a fiber-optic probe and monitoring system
   using DUVAS to provide fast, cost-effective in situ sampling of
   groundwater to identify its contaminants. At the same time, Roger
   Jenkins of the Analytical Chemistry Division is developing an
   arrayed multisorbent sampler--an array of tubes packed with layers
   of various materials that adsorb volatile organics--for in situ
   collection of volatile species at depths up to 38 m (125 ft). An
   example of such an organic pollutant is TCE, a solvent that had
   been widely used to remove grease from metal. The samplers will
   provide temporally and spatially resolved chemical information
   concerning the impact, effectiveness, and zone of influence of
   candidate remediation technologies.    
   
   Considerable time and money can be saved by identifying the
   technologies already available and establishing procedures for
   their use. Wayne Griest, Gary Sega, and Bob Schenley, all of the
   Analytical Chemistry Division, are adapting analytical methods
   already approved by regulatory agencies to the characterization of
   mixed wastes and radioactive environmental samples. 
   
   
   BIOREMEDIATION    
   
   A number of hard-to-degrade volatile organic compounds, such as
   TCE, have been identified as groundwater and soil contaminants at
   DOE sites. These contaminants are of particular concern not only
   because of their potential toxicity but also because of their
   movement through soils as vapors and in water. New technologies are
   needed to remove these contaminants from groundwater and soil and
   to safely dispose of them.    
   
   For example, the popular method of air stripping results either in
   the discharge of TCE to the atmosphere or its capture on activated
   carbon, which itself must then be disposed of. In either case, the
   TCE is not actually destroyed. A more viable solution seems to be
   bioremediation, which is based on the use of organisms to destroy
   the contaminant at the site, thus avoiding the risks to worker
   safety of handling, transporting, treating, or storing contaminated
   residuals.    
   
   Two types of contaminants, perchloroethylene (PCE) and PCB, are
   effectively nondegradable under aerobic (oxygen-rich) conditions,
   but they may be broken down into harmless substances in an
   anaerobic (oxygen-free) environment. At least two OTD projects at
   ORNL are focused on developing techniques to break down these
   chemicals in anaerobic environments. For instance, Terry Donaldson,
   Thomas Klasson, and Betty Evans, all of the Chemical Technology
   Division, are working to identify and cultivate naturally occurring
   anaerobic bacteria that break down PCB molecules by eating and
   digesting them (see the article on "New Waste Technologies" in this
   issue). Likewise, Steve Herbes and Mike Morissey, both of the 
   Environmental Sciences Division, are exploring methods to assist 
   cleanup at the Savannah River Site by anaerobically degrading PCE 
   and other organic compounds resistant to biological treatment using 
   existing commercial processes.    
   
   Because bioremediation approaches that exploit existing bacteria or
   green plants are more socially acceptable than using engineered
   microbes, Barbara Walton and Nelson Edwards, both of the
   Environmental Sciences Division, are studying the effects of
   vegetation on the bioremediation of soils contaminated with TCE and
   PCE. In particular, they will determine whether certain plant
   species and fertilizers speed up the rates at which TCE and PCE
   decompose in soil. Meanwhile, Tony Palumbo of the same division is
   coordinating a soil bioremediation team including scientists from
   both the University of Tennessee and the University of Minnesota.
   They are using innovative methods of monitoring microbial activity
   in the soil to measure the effectiveness of bioremediation of TCE-
   and PCE-contaminated soil and water deep underground at the
   Savannah River Site.
   
   
   TREATABILITY    
   
   Waste retrieval and waste processing currently constitute the
   largest segment of the mission of DOE's Office of Environmental
   Restoration and Waste Management. Current technologies for treating
   contaminated materials to eliminate their toxicity or removing them
   from sites and processing them into a suitable form for shipping or
   disposal are often inadequate and expensive. In situ vitrification
   is one promising technology that instantly destroys many hazardous
   components and immobilizes the remainder by trapping them in a
   block of glass or slag with minimal personnel exposure. Gary Jacobs
   and Brian Spalding, both of the Environmental Sciences Division,
   successfully demonstrated this technique on a trench containing
   radioactive materials.    
   
   A Chemical Technology Division team consisting of Lloyd Youngblood,
   Jr., Zane Egan, Klasson, and Donaldson is adapting previously
   developed techniques for the chemical destruction of
   PCB-contaminated cooling oils and electrical transformer oils to
   the treatment of DOE's mixed wastes. Youngblood is also addressing
   the concern about the integrity of aging tanks containing mixed
   wastes by trying to determine the best method for removing the
   sludge from these tanks before they begin to leak.     
   
   Mixed wastes offer plenty of tough problems for researchers to
   solve. For instance, many aqueous mixed waste streams contain
   concentrations of nitrate that exceed drinking water standards. Al
   Mattus of the Chemical Technology Division is searching for ways to
   chemically reduce the nitrates contained in these mixed waste
   streams, producing gaseous ammonia and achieving acceptable nitrate
   levels. At the same time, Chet Francis of the Environmental
   Sciences Division is hot on the trail of a method for selectively
   removing uranium from soils containing high concentrations of silt
   or clay. Selectively removing the uranium would be much less costly
   than transporting, storing, and monitoring of tons of contaminated
   earth.
   
   
   ROBOTICS    
   
   In the movies, robots are literally able to "boldly go where no one
   has gone before" and save human adventurers from risking life and
   limb. Real-life robots are being developed at ORNL and elsewhere to
   help reduce or eliminate the risks of exposing personnel to
   radioactive or hazardous wastes. Researchers are applying the
   principles of robotics to develop servomechanical devices that
   incorporate sensors, computer control, and human-machine interfaces
   for efficient remote operations under hazardous conditions and for
   improvements in productivity. Typically, a robot possesses
   sufficient autonomous control capability to perform many of its
   functions automatically, but more difficult tasks are supervised
   and guided by a human operator who is remotely located--out of
   harm's way.     
   
   ORNL researchers are focusing on developing a practical robotics
   technology to reduce the hazards and costs of cleaning up DOE
   sites. The work is being carried out by a research team headed by
   Bill Hamel, who also serves as one of the National Robotics Program
   coordinators. This team forms an important part of the Robotics
   Technology Development Program in OTD. This national robotics
   effort is addressing needs at many DOE laboratories and weapons and
   materials production sites.    
   
   The ORNL team seeks to develop robotic technology for applications
   involving underground storage tanks, buried wastes, waste
   minimization, contaminant analysis automation, waste facility
   operations, and decontamination and decommissioning associated with
   DOE facilities.    
   
   Research efforts in the characterization and remediation of
   underground storage tanks are led by Barry Burks of ORNL's Robotics
   and Process Systems Division. Recently, a team led by Burks
   achieved tremendous success in applying computer-based laser
   imaging techniques to mapping the surface topology of
   radon-emitting uranium ore residue stored in silos at what used to
   be the Fernald Feed Materials Production Center in Ohio. The
   accuracy of the surface maps has enabled workers to precisely apply
   a foot-thick contaminant barrier of low-permeability clay over the
   waste to reduce radon emissions, saving DOE millions of dollars in
   remedial action costs (see the article on "New Waste Technologies
   in this issue).    
   
   ORNL's efforts in remote characterization of buried waste sites are
   being led by Brad Richardson and Mark Noakes, both of the Robotics
   and Process Systems Division. Previous collaborative work with the
   U.S. Army is now being extended toward development of a special
   low-ferromagnetic signature vehicle that will significantly improve
   the performance of subsurface mapping sensors, and a new ORNL-Army
   collaboration is seeking to adapt a military backhoe to remote
   excavation of buried waste trenches and contaminated soils.     
   
   Members of Hamel's team are working on robotics projects with
   researchers at other DOE sites who are supported by the Robotics
   Technology Development Program. These collaborations are expected
   to result in significant progress in applying robotics and remote
   technology to the cleanup of DOE sites. 
   
   
   TECHNOLOGY TRANSFER    
   
   The need to make the world a healthier, cleaner, and safer place to
   live in has motivated people everywhere to join together to solve
   a common problem--cleaning up the environment. Tom Gagnier,
   coordinator of the Office of Technology Development environmental
   technology transfer efforts at ORNL, plays a key role in this
   effort by promoting the sharing of technologies among other federal
   agencies, industries, educational facilities, and international
   communities to improve efficiency, reduce costs, and save time in
   environmental cleanup.     
   
   Tom Mayfield of the Office of Technology Transfer of Martin
   Marietta Energy Systems, Inc., is already heavily involved in at
   least two projects at ORNL that do just that. For instance, ORNL
   scientists led by Brenda Faison of the Chemical Technology Division
   have identified biosorbents--biological tissue that will bind
   metal, removing it from solution--that significantly reduce levels
   of uranium, strontium, cesium, lead, silver, iron, cadmium, and
   copper in contaminated process fluids. The team is now putting
   together a cooperative research and development agreement (CRADA)
   with a U.S. firm to develop biosorbent technology for remediation
   of 14 German sites where uranium mining and milling operations were
   carried out from 1949 until they were closed in 1990. The
   technology employed may also be customized for use at other sites,
   including those in the United States.      
   
   The technical exchange goes both ways. ORNL has entered into a
   collaborative agreement with a laboratory in Germany and several
   other DOE facilities in which ORNL personnel led by Robert Siegrist
   will have the opportunity to study unique technologies developed at
   the University of Karlsruhe in Germany, including a groundwater
   well system used to manipulate and treat contaminated soil and
   groundwater and an in situ biotechnology treatment system. In
   addition, the parties involved will study other approaches and
   technologies that have potential applications in both
   countries.Integration    
   
   Somehow, all of these diverse activities have to be brought
   together. To make sure that important information does not fall
   through the cracks, the ORNL team must interact not only with our
   counterparts at the other Energy Systems sites but also with our
   colleagues throughout the DOE complex. In addition, someone must
   make sure that the research being conducted at ORNL is actually
   implemented in the field. These tasks all fall under the
   jurisdiction of the Office of Waste Research and Development
   Programs, directed by Tony Malinauskas with the aid of Norm
   Cutshall and Jan Pruett. The goal of this office is to ensure that
   ORNL becomes a valuable source of model technologies for improving
   the economics and effectiveness of DOE's waste management and
   environmental restoration efforts. 
   
   
   BIOGRAPHICAL SKETCH
   
   Diedre Falter is completing a year-long assignment in the Waste
   Research and Development Program Office at ORNL, where one of her
   first assignments was to write this article for the Review. After
   working as a laboratory supervisor at Transducer Research, Inc., of
   Naperville, Illinois, and receiving her B.S. degree in engineering
   physics from Murray State University in 1986, she joined ORNL's
   Instrumentation and Controls (I&C) Division. There she helped
   develop detectors for use in radiation detection, genome
   sequencing, radiometry, and high-temperature thermometry. She was
   project leader of a team that received a 1990 Martin Marietta
   Energy Systems Technical Achievement Award for development of a
   microminiature infrared transmitter. As a result of that work, she
   was awarded her first patent. She has spent several years
   coordinating precollege (K-12) activities and internships for the
   I&C Division. Her husband is an engineer in the I&C Division. 
   
   
   Diedre Falter
   
   (keywords: waste management, hazardous waste)


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   Date Posted:  2/7/94  (ktb)